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The reliability of fingerprint pore area in personal identification(University of WolverhamptonSchool of Applied Sciences, University of Wolverhampton, 2008)Reproducibility of third level fingerprint detail is important in personal identification. The effect of different substrates on the reproducibility of pore dimensions in inked reference fingerprints was investigated. Photomicrographs of reference prints were taken and pore area was measured repeatedly using appropriate software. Reproducibility of pore area was also studied in latent prints. Latent prints were deposited on chosen absorbent and non-absorbent surfaces and developed using Cyanoacrylate and Ninhydrin to determine pore area reproducibility. Photomicrographs of ridged skin were captured directly by focusing under microscope and pore area reproducibility in these images was studied. Live scans were also included in the study to see if pore area can be relied upon in live scans at 500ppi (pixels per inch). Results revealing best third level detail in inked prints were achieved by deposition onto a variety of non-absorbent substrates but inter-print variation indicated that pore area in inked prints deposited onto paper substrates cannot be used reliably in personal identification. In case of latent prints, variation was greater than normal acceptable limits suggesting that pore area is not reproducible in latent prints developed using Cyanoacrylate and Ninhydrin techniques. Results of direct microscopic images also showed too great inter-image variation which has further supported the unreliability of pore area as a tool in personal identification. Live scans at 500ppi did not prove to be useful in providing good pore detail for study. This study casts doubt on the use of pore area as a reliable identification tool in personal identification and suggests raising the scanning resolution to study pore detail in live scans.
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Latent fingermark pore area reproducibility.(Amsterdam: Elsevier., 2008)The study of the reproducibility of friction ridge pore detail in fingermarks is a measure of their usefulness in personal identification. Pore area in latent prints developed using cyanoacrylate and ninhydrin were examined and measured by photomicrography using appropriate software tools. The data were analysed statistically and the results showed that pore area is not reproducible in developed latent prints, using either of the development techniques. The results add further support to the lack of reliability of pore area in personal identification.
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Development of high-performance liquid chromatographic fingerprints for distinguishing Chinese Angelica from related umbelliferae herbs.(Elsevier, 2005)A high-performance liquid chromatographic (HPLC) fingerprint of Chinese Angelica (CA) was developed basing on the consistent chromatograms of 40 CA samples (Angelica sinensis (Oliv.) Diels). The unique properties of this HPLC fingerprints were validated by analyzing 13 related herbs including 4 Japanese Angelicae Root samples (JA, A. acutiloba Kitagawa and A. acutiloba Kitagawa var. sugiyame Hikino), 6 Szechwan Lovage Rhizome samples (SL, Ligusticum chuanxiong Hort.) and 3 Cnidium Rhizome samples (CR, Cnidium officinale Makino). Both correlation coefficients of similarity in chromatograms and relative peak areas of characteristic compounds were calculated for quantitative expression of the HPLC fingerprints. The amount of senkyunolide A in CA was less than 30-fold of that in SL and CR samples, which was used as a chemical marker to distinguish them. JA was easily distinguished from CA, SL and CR based on either chromatographic patterns or the amount of coniferyl ferulate. No obvious difference between SL and CR chromatograms except the relative amount of some compounds, suggesting that SL and CR might have very close relationship in terms of chemotaxonomy. Ferulic acid and Z-ligustilide were unequivocally determined whilst senkyunolide I, senkyunolide H, coniferyl ferulate, senkyunolide A, butylphthalide, E-ligustilide, E-butylidenephthalide, Z-butylidenephthalide and levistolide A were tentatively identified in chromatograms based on their atmospheric pressure chemical ionization (APCI) MS data and the comparison of their UV spectra with those published in literatures.
